IP 592 Determination of Lead, Nickel, Chromium, Copper, Zinc, Arsenic, Cadmium, Thallium, Antimony, Cobalt, Manganese and Vanadium in Burner Fuels Derived from Waste Mineral Oils - Inductively Coupled Plasma Mass Spectrometry Method

“IP 592 Determination of lead, nickel, chromium, copper, zinc, arsenic, cadmium, thallium, antimony, cobalt, manganese and vanadium in burner fuels derived from waste mineral oils - Inductively coupled plasma mass spectrometry method” published by the Energy Institute among the IP test methods. The standard describes a procedure for determining, by inductively coupled plasma mass spectrometry, the concentration of lead, nickel, chromium, copper, zinc, arsenic, cadmium, thallium, antimony, cobalt, manganese and vanadium in burner fuels derived from waste mineral oils.

This procedure delivers elemental concentrations and internal standards to the instrument generally in the range of 1-50 ng/g. Both higher and lower concentrations of elements in samples can be measured by this method. Lower concentration limits depend on the sensitivity of the tester, the dilution factor, and the cleanliness of the reagents and equipment used for sample digestion. High concentration limits are determined by multiplying the sample dilution factor by the maximum concentration of the analyte used for calibration.

Waste mineral oils are obtained by extracting or processing crude oil. Waste mineral oils are produced by refineries, waste oil-containing lagoons, terminals, drilling operations, ore processing, waste reception facilities and crude oil tank bottom sludges and processable waste oil-derived oils. This type of waste has a highly variable characteristic. Today, large companies offer environmentally friendly solutions with three-phase decanters and separators for the separation or recovery of such waste.

After waste mineral oils are taken into storage tanks, they are generally passed through the following phases. It is heated to 50-70 degrees for a certain holding time. Free water, physically separated from the waste, is taken into the retention phase. Upon removal of free water from the waste storage tanks, the water-oil mixture is pumped and fed to the decanter. The solid phase is separated by the decanter. Then, the product separated from the solid phase is heated to 85-90 degrees and fed to the separator. The oil phase is recovered with the separator and the effluent phase is transferred to the treatment plant. Since the solid phase separated in the previous stage has a high calorific value, it is transferred to disposal facilities or incineration.

Components that can be obtained from mineral oil are: petroleum, aviation gasoline, gasoline, diesel, kerosene, naphthalene, lubricating oil and tar.

Mineral oils are refined petroleum-based hydrocarbons. Mineral oils are a combination of paraffin, naphthenes and aromatic oils. A wide variety of mineral oil compositions are used in cutting and grinding fluids. Lubricating properties have been modified for certain applications using additives. A wide variety of additives are used for different purposes. Extreme pressure additives are added to improve lubricating properties. Mineral oils have lower lubrication performance than synthetic oils.

Waste oil is harmful to the environment and some, such as used motor oils, can cause cancer, so it needs to be managed carefully.

The burner is a device that ensures that fuel mixes with air at the optimum rate and burns under complete control. Industrial burner is an important product for heating technologies. Combustion is defined by the release of heat resulting from the chemical reaction of combustible components in the fuel with oxygen. When the fuel reacts with oxygen, combustion occurs and heat energy and light are released. The main goal is to reach heat after converting chemical energy into thermal energy.

Among the numerous testing, measurement, analysis and evaluation studies carried out for businesses in various sectors, our organization, with its trained and expert staff and advanced technological equipment, has established the following standards: "IP 592 Lead, nickel, chromium, copper, zinc, arsenic in burner fuels derived from waste mineral oils". It also provides testing services defined in the standard "Determination of cadmium, thallium, antimony, cobalt, manganese and vanadium - Inductively coupled plasma mass spectrometry method".